speedwave XPERT – Microwave Pressure Digestion System

plus d'images

Description

Sample preparation at the highest level 

  • Reliable digestions thanks to innovative sensor technologies  
  • Outstanding lifetime of vessels
  • Maximum safety and increased user comfor

Microwave-assisted pressure digestion is used as a sample preparation technique for reliable elemental analysis in routine and research laboratories alike. speedwave XPERT is a universally applicable microwave digestion system for the preparation of organic and inorganic sample materials that impresses with its reliability, safety, and economy.

Reliable, durable, and economic

speedwave XPERT sets new standards with its innovative sensor technology and high-quality components. Real-time temperature and pressure monitoring takes place contactless for all vessels, which can be removed individually after digestion. The vessels of speedwave XPERT have an outstanding lifetime of up to 10,000 digestion cycles. Low material wear and protection of the vessels against damage by optical pressure and temperature control also ensure that you can significantly reduce your running costs in sample preparation.

  • No cross-contamination due to minimal surface porosity of TFM-PTFE vessels
  • Homogenous distribution of microwave radiation due to the round design of the oven chamber
  • Permanent pressure and temperature control by optical sensors

Maximum Operational Safety and High Application Variety

Working under demanding conditions requires an absolutely reliable system. The pressure-resistant furnace with an electrically locked swiveling lid is equipped with an integrated exhaust system to prevent reaction gases from escaping. The furnace chamber is permanently ventilated. To reduce safety risks from irregular heating, a monitoring of the reaction parameters pressure and temperature is of particular importance. Thanks to real-time monitoring of the internal vessel pressure automatic regulation and, if necessary, shutdown of processes, takes place in case of exothermic reactions.

  • Top-loading concept and electronic lid lock
  • Permanent ventilation of the oven chamber and removal of generated acid fumes by the fume collection system
  • Automatic regulation in case of exothermic reactions

The speedwave XPERT vessels are manufactured with the highest quality standards. They are made from high quality TFM-PTFE and impress through reliability and an outstanding lifetime. Vessel volumes cover a wide range, from 40 to 100 mL. You can choose between four vessel options, offering maximum flexibility for digestions up to 260 °C and 100 bar. The vessels comprise only few individual parts. They are opened and closed manually and without additional tools. When the vessels are opened, the remaining pressure is released safely and controlled. All vessels are equipped with a rupture disc, which breaks when the overpressure exceeds the tolerance level. This allows an immediate termination of the digestion run in case of exothermic reactions. Thus, expensive consequential damage is avoided. Additional liner systems expand the field of applications of existing vessel types. The vessels can be equipped with inserts to support digestion of small sample quantities or complex samples.

Pressure monitoring (Optical Pressure Control OPC) involves optical detection of the internal vessel pressure. The patented technology uses a glass ring, on which the internal pressure acts as a sensor element. Increases in pressure are reflected by changes to the optical characteristic of the glass. The sensor element located in the screw cap of the digestion vessel records these changes and shows the pressure individually for each sample. The optical detection of the vessel surface temperature (Optical Temperature Cut-Off OTC) increases safety and lifetime of the digestion vessels and allows for an individually programmable upper temperature limit. The optical detection of each sample temperature (Direct Infrared Control DIRC) is a patented temperature measurement process, here as well, an infrared thermometer is used for contactless control in all vessels instead of just one reference vessel. Thanks to the optical pressure control in every vessel, exothermic reactions are detected early and the process is automatically regulated or stopped by speedwave XPERT.

  • Real-time monitoring
  • Minimization of the risk of contamination
  • Easy handling

The innovative design of speedwave XPERT builds a connection of convenience and function. A special feature of the microwave digestion system is its top-loading concept. The swiveling lid allows the vessels to be easily loaded from above, providing optimal operator comfort. speedwave XPERT can be operated via a 7" touch controller with a graphical user interface, as well as via mobile devices or PC/laptop.

Données techniques

Technical Data

speedwave XPERT – Microwave Pressure Digestion System

Dimension (width x depth x height)

Order number: 819-5005000-2

880 mm x 645 mm x 480 mm

Logiciel

speedwave XPERT can be operated via a 7" touch controller
with a graphical user interface, as well as via mobile devices or PC/laptop.

speedwave XPERT Software – pre-installed standard software for full control included, for 21 CFR part 11 compliance please select 819-5005011

Product

Required

Included

speedwave XPERT - Microwave Pressure Digestion System (819-5005000-2)

Accessoires

Accessories and Consumables

Accessory

Order number

Concentration/Evaporation unit for CX 100

819-5004820-0

Turntable ring speedwave XPERT –
for DAP-60/100 and DAK-100

819-5005148

CX 100 Opening station

819-5303625-0

 

 

Forming tool CX 100

819-5302026-0

Forming tool PL 100

819-5303751-0

Forming tool PM 40

819-5303437-0

Forming tool PM 60

819-5014612-0

 

 

speedwave XPERT Start DAP60X samples –
12x 60 mL, 40 bar *

819-5005060

speedwave XPERT Start DAK100X samples –
8x100ml, 100bar *

819-5005100

speedwave XPERT Start DAK100X OPC-samples –
8x100ml, 100bar *

819-5005101

speedwave XPERT Start DAP100X OPC-samples –
12x100mL 25 bar/ 40 bar *

819-5005103

speedwave XPERT Start DAP100X samples –
12x100 ml, 25 bar/ 40 bar *

819-5005102

speedwave XPERT Start DAP40X samples –
24 x 40 ml, 40 bar *

819-5005040

speedwave XPERT Start DAP60X OPC-samples –
12x60ml, 40bar *

819-5303277-0

* necessary to operate

 

Consumables

Order number

Name

Rupture disc Special for PM 60 vessels, 50 bar,
stainless steel (SS316), set of 20 pieces

419-5303740-0

Cap for CX 100-vessel with pressure control

819-5004780-0

Cap for PM 40 vessel
with pressure control

819-5003790-0

Cap for vessels
with pressure control

819-5003580-0

Cap insert for closure caps
with pressure control (RPM)

419-5303567-0

PM 40 Cap
without pressure control
for PM 40 vessel made of TFM

419-5303433-0

Cap insert for closure caps CX 100
with pressure control (RPM)

419-5304707-0

CX 100 Vessel complete

819-5004720-0

CX 100 Vessel complete RPM

819-10000002-0

CX 17 Insert made of TFM, 17 ml

419-5303283-0

CX 17 pressure jacket

419-5303282-0

CX 17 Spacer ring made of PTFE

419-5303428-0

Cap insert for closure caps CX-100
with pressure control (OPC)

819-5304763-0

Enlargement insert CX 100

819-5303277-0

Enlargement insert PH 30

819-5303661-0

Enlargement insert PL 100

819-5303299-0

Enlargement insert PM 60

819-5303278-0

Fixation screw for lip seal ring

419-5302963-0

Forming System 6-fold CX 100

819-5303386-0

Forming System 6-fold PL 100

819-5303275-0

Forming System 6-fold PM 60

819-5303385-0

Forming system TOPwave

819-5303245-0

Prisma RPM Glass prism for closure caps
with pressure control (RPM)

419-5303573-0

CX 100 Glass-Ring for closure caps CX 100
with pressure control (RPM)

419-5304882-0

Knurled nut for exhaust tube
of gas collection system

419-5004110-0

Lid for CX 100
made of TFM, set of 5 pieces

419-5308060-0

CX 17 Lid for CX 17 made of TFM,
set of 4 pieces

419-5303485-0

Lid for PH 30
made of TFM, set of 10 pieces

419-5709024-0

Lid for PL 100
made of TFM, set of 5 pieces

419-5300005-0

Lid for PM 60 made of TFM,
set of 5 pieces

419-5014617-0

Lid for QX 20 / QX 22
made of TFM, set of 10 pieces

419-5014420-0

Lid for QX 20 / QX 22
made of TFM, set of 4 pieces

419-5014414-0

CX 100 Liner insert for pressure vessel CX 100
made of TFM, 100 ml, 100 bar

419-5303287-0

Lip-seal ring for the gas collection system

419-5302962-0

Marble granulate for evaporation unit

419-5014622-0

O-Ring RPM 25 x 3 mm for closure caps
with PM 40 pressure control (RPM)

419-5306386-0

O-Ring RPM (Viton)

419-5304101-0

PEEK-Rung nut for CX 100 closure cap

419-5303296-0

PL 100 Vessel complete

819-5003630-0

PL 100 Vessel complete RPM

819-5003632-0

Lid for PM 40 made of TFM, set of 10 pieces

419-5303446-0

PM 40 Vessel complete

819-5003270-0

PM 60 Vessel complete

819-5003560-0

PM 60 Vessel complete RPM

819-5003559-0

Polarisation foil for prism RPM, set of 24 pieces

419-5303588-0

PTFE Adapter piece CX 17 in PL 100

419-5303389-0

QX 20 Centring sleeve made of PTFE

419-5014433-0

Knurled screw for closure caps
with pressure control (RPM)
for PH30/PM60/PL100

419-5303571-0

Rupture disc for CX 100 made of Titanium,
100 bar, set of 10 pieces

419-5308040-0

Rupture disc for PM 40 made of aluminium,
40 bar, set of 25 pieces

419-5303445-0

Rupture disc for QX 20 / QX 22 made of Monel,
100 bar, set of 5 pieces

419-5014410-0

Rupture disc Special PM 60 (reinforced),
set of 25 pieces

419-5303065-0

Rupture disc standard PH 30 and PL 100,
set of 25 pieces

419-5014616-0

Screw cap for CX 100
without pressure measurement

419-5004740-0

Set caps for CX 100-vessels
without pressure control

819-5004730-0

Set caps for CX 100-vessels
with pressure control

819-5004790-0

Set caps for vessels without pressure control

819-5003540-0

Set caps for vessels with pressure control

819-5003590-0

PL 100 Special lid with integrated TFM rupture
disc for PL 100

419-5046170-0

Special lid with integrated TFM rupture
disc for PM 60

419-5046180-0

tool kit CX-100 RPM-screw caps

419-10000013-0

Vent-tube set 2 m

419-5303227-0

Vent-tube set 4 m

419-5303537-0

Connecting tube to gas collection system /
integrated suction system (without nut)

419-5303508-0

CX 100 Vessel bottom made of TFM

419-5003279-0

Vessel bottom PH 30 made of TFM

419-5003605-0

PL 100 Vessel bottom made of TFM

419-5003672-0

Vessel bottom PM 40 made of TFM

419-5003447-0

Vessel bottom PM 60 made of TFM

419-5003603-0

Weighing cup (2.0 ml, Set of 12 pieces)

419-5303612-0

CX 100 Blind plug for turntable
to seal the gas collection system

419-5302817-0

connection fitting for L100, PM60

419-5303566-0

Consumables CX 100 for vessels
without pressure control

819-5303955-0

Consumables PL 100

819-5303953-0

Consumables PM 40

819-5303448-0

Consumables PM 60

819-5303952-0

Consumables set CX100 for vessel
with pressure control

819-5303965-0

CX 100 ceramic pressure jacket (white-new)

419-5303284-0

Evaporation unit CX 100 evaporation lid

419-5303825-0

Nut for connecting tube
to gas collection system/ integrated suction system

419-5302811-0

Neutralisation Unit - for neutralisation of fumes

819-5005055

Cap without pressure control
for PH 30 / PM 60 /
PL 100 vessel made of TFM

419-5303563-0

* necessary to operate

 

 

Téléchargements

  • Brochure speedwave XPERT (English)
    .pdf | 4.06 MB

    speedwave XPERT is a universally applicable microwave digestion system for the preparation of organic and inorganic sample materials that impresses with its reliability, safety, and economy.

The newsletter of Analytik Jena frequently keeps you posted about:

Sign up here